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　　哈希HACH-NPW-160H总磷-总氮水质在线分析仪 使用手册-操作说明书.pdf

　　哈希HACH-NPW-160H总磷-总氮水质在线分析仪 使用手册-操作说明书.pdf

　　使用说明书 总磷/总氮水质在线H 型 ●请在使用前仔细阅读本使用说明书，正确使用。 ●请将本使用说明书交给实际操作产品的人。 手册号:NPW-AA77504C NPW-160H 型 前言 前言 (a) 非常感谢您购买本产品。本“总氮·总磷自动测定装置 NPW-160H 型” （下称“产品”）的目的 是自动测量总氮和总磷浓度，以应对工厂、处理场等事业所的排水监视。 (b) 本产品的主要规格见下表。有关规格详情，请参见[9.规格和动作说明] 。此外，测定范围因 嵌入的检测器的单元池长度而异。根据订单规格在产品上嵌入单元池长度的检测器，在单元 池长度 10mm 以外的检测器贴有标签，注明“单元池长度 20mm”或“单元池长度 5mm”。 主要规格 规格项目 内 容 测定对象成分 水中的总氮(TN)浓度、总磷(TP)浓度 测定范围 10mm 池 TN ：最小0～5 mg/L，最大0～50 mg/L TP：最小0～2 mg/L，最大0～20 mg/L 20mm 池 TN ：最小0～2 mg/L，最大0～25 mg/L TP：最小0～0.5 mg/L，最大 0～10 mg/L 5mm 池 TN :0～100 mg/L TP：最小0～2 mg/L，最大0～20 mg/L 测定周期 1 次测定/1 小时。 间歇连续。 利用日程设定功能，可任意设定 1 天（24 小时）的测定类别。 测定类别：不测定、水样测定、零水测定、标准液测定。 (c) 本装置的废液是混合了试剂类与水样的溶液，是 pH1.0 以下的強酸性溶液。 【重要】· 废弃时请进行合适的处理，或者委托专业的处理业者。 (d) 以下因素可能使产品显示或输出异常的测定值。建议预先建立不会造成相关设备损坏的系 统。 ·检测部分老化及损伤、电缆绝缘不匹配等产品故障。 ·腐蚀性气体引起的电气系统故障。 ·不当运行条件的设定及校对操作。 ·周围干扰、接地不良等电气故障。 ·其他意外情况。 (e) [安全注意事项]记载了非常重要的内容，请务必仔细阅读。 (f) 请安排经过相关培训的人员进行产品的操作。此外，修理等技术服务请交由经过本公司技术 培训或具备同等技术能力的人员执行。 (g) 请务必遵守贵国及贵地区的法律法规，操作（包括废弃）本产品。 - 1 - NPW-160H 型 安全注意事项 安全注意事项 (1) 标记含义 在使用说明书中与警告相关的符号及其含义如下所示。此外，除表示可能会出现的危险和损 坏外，产品标签等的警告标识（ ：一般提示图形符号）兼具“参见使用说明书”的含义。 ： 表示不当操作可能会导致重伤甚至死亡的危险程度。 警告 所谓重伤是指因失明、烫伤（高温和低温）、触电、骨折、中毒等留下后遗症 及入院治疗、长期到医院门诊治疗的情况。 ： 表示不当操作可能会导致人员受伤或财产损失的危险、损坏程度。 注意 所谓伤害是指不需要住院或长期到医院门诊的受伤、烫伤、触电。所谓财产损 失是指房屋、家庭财产及家畜、宠物、设备、器材等扩大损失（产品自身以外 发生的损失）。 【重要】 ： 表示 及 以外有关的重要事项。表示防止产品主体破损、数据损坏、 时间浪费、维持性能、遵守法律等的事项。 〔备注〕 ： 表示为帮助加深理解而提供的解释、原因、背景、特例等内容。 ＞＞： 表示参考项目。 ① ③…： 表示操作等的项目编号。 (2) 安全遵守事项 警告 燃 气 ● 请勿在存在爆炸性气体、易燃性气体等的场合使用，否则可能引发爆炸、 火灾。 触 电 ● 通电中请勿触摸产品内部的端子。否则可能导致触电。 ● 请务必将接地端子接地，否则电源系统发生故障时可能造成触电。 危险有害物质 ● 使用试剂1 （过硫酸钾）、试剂2(氢氧化钠)、试剂3 （盐酸）、试剂4 （钼 酸铵）时，请务必确认安全数据表（SDS）的内容，操作时务必穿戴防护 器具。 - 2 - NPW-160H 型 安全注意事项 注意 翻 倒 ● 使用本产品之前，请使用基座螺栓等进行固定。移动及存储时，请用绳子 等捆绑以防止翻倒。本产品的重量约为 76kg。翻倒可能会引起危险和损 害。 拆解和改造 ● 请勿拆解、改造使用说明书未说明的部分。否则可能发生损害。 警告标签 ● 当产品上贴的警告标签模糊不清时，请向经销商或本公司销售办事处购买 丢失 新标签，并贴到原来的位置。 (3) 使用说明书的使用 本使用说明书记载有[安全遵守事项]等非常重要的内容。使用方法如下： (a) 使用说明书对产品使用初期及以后的操作、保养及故障诊断都非常有帮助。请将使用说明书 保存在产品附近，以便实际操作产品的人员可随时就地查阅。 (b) 如果使用说明书丢失、污损不清，请向经销商等重新购买。 (c) 为便于理解，在使用说明书、产品上张贴的标签等上，对图形形状及部分界面进行了省略或 抽象化设计。此外，界面示例中的数字等仅表示一个例子。 (d) 本公司保留在未事先通知情况下随时修改产品使用说明书的权利。 (e) 本使用说明书的知识产权归本公司所有。未经公司同意，请勿全部或部分转载。 - 3 - NPW-160H 型 产品保修 产品保修 (1) 保修适用对象 东亚 DKK 株式会社(以下称[本公司])在保修期内对产品的材料及制造提供保修。 (a) 保修期是指自交付用户首日起的一年时间。此外，交货日期不清楚时，以产品铭牌上记载的生产日期 的下一个月起的24 个月为准。 (b) 与本公司之间存在书面的个别合同时，优先遵照个别合同。 (c) 在本书规定的质保期内法律不允许这样的限制时，有时不适用。 (2) 保修失效情况 本保修不适用于以下情况： (a) 因超出本产品规格及使用说明书记载的范围的目的、使用方法导致的直接或间接性故障、损坏等。 (b) 因地震、风暴、水灾、雷击等自然灾害以及事故、火灾、电压异常、盐害、燃气灾害、劳动争议、战 争、恐怖行为、内乱、主管政府所做的处置等不可抗力发生的直接或间接性故障、损坏等。 (c) 未经本公司许可进行修理、改造造成的故障、损坏等。 (d) 购买后应归咎于本公司责任的运输、移动、掉落等原因导致的故障、损坏等。 (e) 电极及易损件（比主体分析仪的保修期短时，遵照各自的质保期。尤其是超过制造后6 个月时，请咨 询本公司或经销商。） (f) 因使用了非本公司制造的易损件、零部件、软件等导致的故障、损坏等。 (g) 因使用非本公司制造的连接设备导致的故障、损坏等。 (h) 产品中保存的数据、设定信息、程序及软件等不应归咎于本公司责任造成的丢失。 (i) 将用户指定的其他公司的产品与本公司产品组合而成的产品(含嵌入本公司产品的产品)(*1) 。此时， 本公司仅对本公司产品负责保修。 (j) 没有遵照本公司提供的使用说明书进行合适的保养的产品。 (k) 无产品铭牌的产品 (但有证据表明是本公司交付的情况除外) 。 (l) 没有进行本公司在交货规格书中指定的设置、配管、配线时。 本公司也不负责本书明确规定的保修以外的任何保修。本公司明确声明不承担法律上默许适用的性能的保证、 对特定目的的性能保证等义务。 救助的限制：保修期内发现故障时，由本公司或本公司授权的经销商根据自身的裁量修理故障，或者更换零部件 或产品，或者退还产品的货款。 本公司承担上述保修责任。 损害赔偿的限制：无论何种情形，本公司也不对违反保修义务、过失、严重责任等造成的附带损害或间接损害承 担赔偿义务。 (3) 其他 (a) 本产品的保养零部件(*2)向用户供货期限为停产后五年 (*3) 。 (b) 故障、损坏等的原因应由本公司技术人员评定。 (c) 修理工作请委托本公司或当地经销商。 *1：其他公司产品的保修单由用户负责管理。 *2：所谓保养零部件是指包括维持产品正常运行所必需的零部件。 *3：无法购买，无替代品时，也有可能不到五年。 - 4 - NPW-160H 型 阅读方法指南 阅读方法指南 请根据理解产品概要、如何开始操作等目的，参见本使用说明书的必要项目。图中带圆圈的 数字主要是指参见项目和顺序。 目 的 启动 进行个别操 进行保养检 理解产品的 确认设置 ） （开启 作 查或故障处 概要 置措施 章 ●前言 ●安全注意事项 1.构成 2.运行前准备 3.运行和停止 4.校 对 5.不同目的的操作 6.保 养 7.故障处理措施 8.纯水供给 9.规格和动作说明 10.设 置 11. RS485Modbus通信规格 - 5 - NPW-160H 型 目 录 目 录 ●前言 ········································································································································ 1 ●安全注意事项 ··········································································································· 2 (1) 标记含义…2 (2) 安全遵守事项…2 (3) 使用说明书的使用…3 ●产品保修 ························································································································· 4 ··········································································································· 5 ●阅读方法指南 1. 构 成 ····························································································································· 12 1.1 各部分的名称 ···································································································· 12 (1) 测定系统示例…12 (2) 主要部分的名称…12 (3) 操作部分的名称… 14 1.2 界面的功能 ········································································································ 15 (1) 工序界面…15 (2) 界面组…17 (3) 操作界面路线. 运行前准备 ·········································································································· 19 2.1 设置确认和冲洗 ······························································································· 19 (1) 设置、规格、阀门位置等的确认…19 (2) 配管冲洗…20 2.2 检测器的安装 ···································································································· 21 2.3 溶液等的调制和填充 ····················································································· 22 (1) 测定模式和要准备的溶液等…22 (2) 试剂 1…23 (3) 试剂 2…24 (4) 试剂 3…25 (5) 试剂 4…25 (6) 试剂 5…27 (7) 标准校对液…28 2.4 确认夹管阀的软管 ·························································································· 31 3. 运行和停止 ·········································································································· 32 3.1 运行开始 ············································································································· 32 3.2 USB 存储器 ········································································································ 37 (1) USB 存储器的安装…37 (2) USB 存储器的拆卸…38 3.3 试剂泵排气 ········································································································ 39 - 6 - NPW-160H 型 目 录 (1) 自动方法…39 (2) 手动方法…39 3.4 自动测定开始方法的选择 ············································································ 43 (1) 功 能…43 (2) 内置时钟方法…43 (3) 利用 RS485Modbus 通信的方法…43 3.5 参数的确认 ········································································································ 44 3.6 外部输入输出信号的循环检查 ·································································· 48 (1) 外部输入输出信号一览…48 (2) 各信号的循环检查…49 3.7 USB 数据与加工示例 ····················································································· 50 3.8 测定停止与运行停止 ····················································································· 52 (1) 自动测定的正常停止和再启动…52 (2) 自动测定的紧急停止…53 (3) 短期停止运行和再启动…53 (4) 长期停止运行和再启动…54 4. 校对 ································································································································ 55 4.1 校对的种类 ········································································································ 55 ············································································ 57 4.2 自动校对开始方法的选择 (1) 功 能…57 (2) 自动校对开始（外部启动OFF 时）…58 (3) 自动校对开始（外部启动ON 时）…58 4.3 手动校对 ············································································································· 59 4.4 自动确认功能 ···································································································· 61 5. 不同目的的操作···························································································· 62 5.1 操作界面 ············································································································· 62 (1) 功 能…62 (2) 水样自动测定…63 (3) 校对液自动测定…65 (4) 正常停止…67 (5) 紧急停止…68 (6) 保养信号的切换…69 5.2 测定值界面 ········································································································ 70 (1) 功 能…70 (2) 测定值等的确认…70 5.3 警报界面 ············································································································· 73 (1) 功 能…73 (2) 异常记录的确认…73 (3) 异常显示的解除…74 5.4 管理界面 ············································································································· 75 5.5 零点校对界面 ···································································································· 76 - 7 - NPW-160H 型 目 录 (1) 功 能…76 (2) 零点校对记录的确认…77 (3) 手动零点校对的开始…77 5.6 标准校对界面 ···································································································· 79 (1) 功 能…79 (2) 标准校对记录的确认…80 (3) 手动标准校对的开始…80 5.7 个别动作界面 ···································································································· 82 (1) 功 能…82 (2) 操作步骤…83 (3) 紧急停止时洗涤的执行…84 (4) 纯水引进的执行…84 (5) 替换空气的执行…84 (6) 加热分解槽洗涤的执行…84 (7) 试剂注入的执行…84 (8) SH 检查的执行…85 (9) 试剂初期化的执行…85 (10) 试剂泵替换空气的执行…85 5.8 参数界面 ············································································································· 86 (1) 功 能…86 (2) 参数设定值的确认…88 (3) 参数设定值的更改…88 (4) A01— 日期…90 (5) A02—时刻…90 (6) A03—测定开始时间…90 (7) A04、A05—控制信号…91 (8) A06、A07—测定范围…91 (9) A08—机器 ID…92 (10) A09—产品 NO…92 (11) B01—校对模式…92 (12) B02、B04—校对次数…92 (13) B03、B05—删除次数…92 (14) B06— 自动校对周期…92 (15) B07— 自动校对开始时刻…93 (16) B08—下次校对日…93 (17) B09、B10—标准液浓度…93 (18) B11～14—零、标准系数…94 (19) C01―SV3 洗涤间隔…94 (20) C02—SV3 洗涤浓度…95 (21) C03 润洗次数…95 (22) C04 自动审查模式…95 (23) C05 自动审查零次数…95 (24) C06 自动审查标准次数…95 (25) C07 自动审查周期…96 - 8 - NPW-160H 型 目 录 (26) C08 自动审查开始时刻…96 (27) C09 下次自动审查日…96 (28) D01、02、04、05—修正系数…96 (29) E01～04—浓度警报…97 (30) E05～09—试剂剩余…97 (31) F01—测定模式…98 (32) F02—外部启动…98 (33) F03～06—稀释倍率…99 (34) F07—趋势模式…99 (35) G01～06—检测器参数…99 (36) H01～24—预定计划表…100 (37) I01～09—接点输出…100 5.9 输入监视器界面 ····························································································· 101 (1) 功 能…101 (2) 动作状况的确认…102 5.10 检测器监视器界面 ························································································ 103 (1) 功 能…103 (2) 透过电压的确认…104 5.11 检查模式界面 ·································································································· 105 5.12 步骤动作界面 ·································································································· 106 (1) 功 能…106 (2) 步骤动作执行…106 5.13 输出检查界面 ·································································································· 108 (1) 功 能…108 (2) 电磁阀等的动作确认…109 5.14 A/D 输入校对界面 ························································································ 111 (1) 功 能…111 (2) A/D 输入校对 … 112 5.15 D/A 输出校对界面 ························································································ 115 (1) 功 能…115 (2) D/A 输出校对 … 116 5.16 D/A 测试界面 ································································································· 119 (1) 功 能…119 (2) 传输输出的测试…120 5.17 技术服务用按键的锁定解除 ····································································· 122 5.18 版本界面 ··········································································································· 124 (1) 功 能…124 (2) 版本的确认…125 6. 保养 ······························································································································ 126 6.1 保养一览 ··········································································································· 126 6.2 附件与备件 ······································································································ 129 6.3 各种储罐 ··········································································································· 133 - 9 - NPW-160H 型 目 录 (1) 检 查…133 (2) 溶液的补充和罐的清洗…133 6.4 废液罐 ················································································································ 136 (1) 检 查…136 (2) 废液的回收和软管的更换…136 (3) 废液的处理…137 6.5 采水路径和接液槽 ························································································ 138 (1) 采水路径的检查…138 (2) 接液槽的流量调整…138 (3) 接液槽的清洗和零部件更换…139 (4) 软管更换(接液槽～送液泵 P6) … 140 6.6 电磁阀 ················································································································ 142 (1) 电磁阀的类型和检查…142 (2) 更换…143 6.7 夹管阀 ················································································································ 144 (1) 夹管阀的一览和检查…144 (2) 更换…144 6.8 送液泵 ················································································································ 146 (1) 检 查…146 (2) 泵软管的更换…147 (3) 送液泵的更换…149 6.9 气泵 ····················································································································· 151 (1) 检 查…151 (2) 气泵的更换…151 6.10 试剂泵 ················································································································ 153 (1) 检 查…153 (2) 注射器配套元件等的更换…154 (3) 试剂泵用电机的更换…160 6.11 纯水泵 ················································································································ 163 (1) 检 查…163 (2) 润滑脂涂抹…164 (3) 注射器组件的清洗和更换…166 6.12 电磁阀块 ··········································································································· 171 (1) 检 查…171 (2) 电磁阀块的保养…171 6.13 加热分解槽 ······································································································ 174 (1) 检 查…174 (2) 加热器等的更换…176 (3) 加热软管的更换…179 6.14 反应槽 ················································································································ 180 (1) 检 查…180 (2) 反应槽的清洗和 O 形环的更换…182 (3) 软管的更换和插入深度的调整…183 (4) 5 号软管插入深度的调整…185 - 10 - NPW-160H 型 目 录 6.15 检测器 ················································································································ 187 (1) 检 查…187 (2) 流动池的清洗…188 (3) 光源灯的确认和更换…190 7. 故障处理措施 ··············································

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